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Uranyl Perchlorate, UO2(ClO4)2

Uranyl Perchlorate, UO2(ClO4)2.6H2O, is prepared by adding perchloric acid to a solution of potassium uranate, filtering off the precipitated potassium perchlorate, and evaporating the filtrate over phosphorus pentoxide. It forms yellow prismatic crystals, which melt at 90° C., and at 100° C. lose water, yielding the tetrahydrate, UO2(ClO4)2.4H2O.

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